Marc-Olivier Ebert: Catalogue data in Autumn Semester 2016 |
Name | Dr. Marc-Olivier Ebert |
Address | Lab. für Organische Chemie ETH Zürich, HCI E 315 Vladimir-Prelog-Weg 1-5/10 8093 Zürich SWITZERLAND |
Telephone | +41 44 633 47 26 |
Fax | +41 44 632 14 75 |
marc-olivier.ebert@org.chem.ethz.ch | |
Department | Chemistry and Applied Biosciences |
Relationship | Lecturer |
Number | Title | ECTS | Hours | Lecturers | |
---|---|---|---|---|---|
529-0051-00L | Analytical Chemistry I | 3 credits | 3G | D. Günther, M.‑O. Ebert, R. Zenobi | |
Abstract | Introduction into the most important spectroscopical methods and their applications to gain structural information. | ||||
Objective | Knowledge about the necessary theoretical background of spectroscopical methods and their practical applications | ||||
Content | Application oriented basics of organic and inorganic instrumental analysis and of the empirical employment of structure elucidation methods: Mass spectrometry: Ionization methods, mass separation, isotope signals, rules of fragmentation, rearrangements. NMR spectroscopy: Experimental basics, chemical shift, spin-spin coupling. IR spectroscopy: Revisiting topics like harmonic oscillator, normal vibrations, coupled oscillating systems (in accordance to the basics of the related lecture in physical chemistry); sample preparation, acquisition techniques, law of Lambert and Beer, interpretation of IR spectra; Raman spectroscopy. UV/VIS spectroscopy: Basics, interpretation of electron spectra. Circular dichroism (CD) und optical rotation dispersion (ORD). Atomic absorption, emission, and X-ray fluorescence spectroscopy: Basics, sample preparation. | ||||
Lecture notes | Script will be for the production price | ||||
Literature | - R. Kellner, J.-M. Mermet, M. Otto, H. M. Widmer (Eds.) Analytical Chemistry, Wiley-VCH, Weinheim, 1998; - D. A. Skoog und J. J. Leary, Instrumentelle Analytik, Springer, Heidelberg, 1996; - M. Hesse, H. Meier, B. Zeeh, Spektroskopische Methoden in der organischen Chemie, 5. überarbeitete Auflage, Thieme, Stuttgart, 1995 - E. Pretsch, P. Bühlmann, C. Affolter, M. Badertscher, Spektroskopische Daten zur Strukturaufklärung organischer verbindungen, 4. Auflage, Springer, Berlin/Heidelberg, 2001- Kläntschi N., Lienemann P., Richner P., Vonmont H: Elementanalytik. Instrumenteller Nachweis und Bestimmung von Elementen und deren Verbindungen. Spektrum Analytik, 1996, Hardcover, 339 S., ISBN 3-86025-134-1. | ||||
Prerequisites / Notice | Excercises are integrated in the lectures. In addition, attendance in the lecture 529-0289-00 "Instrumental analysis of organic compounts" (4th semester) is recommended. |