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651-4063-00L  X-ray Powder Diffraction

SemesterHerbstsemester 2016
DozierendeM. Plötze
Periodizitätjährlich wiederkehrende Veranstaltung
KommentarMaximale Teilnehmerzahl: 12

KurzbeschreibungIn the course the students learn to measure X-ray diffraction patterns of minerals and to evaluate these using different software for qualitative and quantitative mineral composition as well as crystallographic parameters.
LernzielUpon successful completion of this course students are able to:
- describe the principle of X-ray diffraction analysis
- carry out a qualitative and quantitative mineralogical analysis independently,
- critically assess the data,
- communicate the results in a scientific report.
InhaltFundamental principles of X-ray diffraction
Setup and operation of X-ray diffractometers
Interpretation of powder diffraction data
Qualitative and quantitative phase analysis of crystalline powders (e.g. with Rietveld analysis)
SkriptSelected handouts will be made available in the lecture
LiteraturALLMANN, R.: Röntgen-Pulverdiffraktometrie : Rechnergestützte Auswertung, Phasenanalyse und Strukturbestimmung Berlin : Springer, 2003.
DINNEBIER, R.E. et al.: Powder Diffraction. Royal Society of Chemistry, Cambridge, 2008. (http://pubs.rsc.org/en/Content/eBook/978-0-85404-231-9)
PECHARSKY, V.K. and ZAVALIJ, P.Y: Fundamentals of Powder Diffraction and Structural Characterization of Materials. Springer, 2009.
Voraussetzungen / BesonderesThe course includes a high portion of practical exercises in sample preparation as well as measurement and evaluation of X-ray powder diffraction data.
Own sample will be analysed qualitatively and quantitatively. Knowledge in mineralogy of this system is essential.
The lecture course is limited to 12 participants.